The analyses presented in this paper include the concentration levels of NO
2 and O
3 measured during 2 successive years in twin cities (Rawalpindi and Islamabad) of Pakistan from November 2009 to March 2011. NO
2 was determined using the passive sampling method, while ozone was determined by Model 400E ozone analyzer. The average NO
2 and O
3 concentration in twin cities of Pakistan was found to be 44?±?6 and 18.2?±?1.24 ppb, respectively. Results indicate that the concentration of NO
2 and O
3 show seasonal variations. Results also depict that NO
2 and O
3 concentration levels are high in areas of intense traffic flow and congestion. Rawalpindi has more elevated levels of NO
2 and O
3 as compared to the Islamabad due to the narrow roads, enclosing architecture of road network and congestion. Climatic variables also influenced the NO
2 and O
3 concentration, i.e., temperature is positively related with O
3, while negatively related with NO
2, relative humidity is directly related with NO
2 and inversely related with O
3, whereas rainfall show negative association with both NO
2 and O
3 concentration. Comparing the results with WHO standards reveals that NO
2 concentration levels at all the sampling points are above the permissible limit, while ozone concentration is still lower than the WHO standards. Thus, there is a need to take appropriate steps to control these continuously increasing levels of NO
2 and O
3 before they become a serious hazard for the environment and people living in those areas.
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